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Chemistry · 9701 · 6 min read · Updated 2026-05-11

Synthetic route planning — CIE A-Level Chemistry

CIE A-Level Chemistry · 9701 · 6 min read

1. Retrosynthetic Analysis Basics ★★☆☆☆ ⏱ 10 min

Retrosynthesis simplifies complex planning problems by reducing the size of the target molecule step-by-step, making it easier to identify viable starting materials and reaction sequences.

Exam tip: Always use retrosynthetic arrows (not standard reaction arrows) for retrosynthetic analysis to earn full marks

2. Selecting Reagents and Conditions ★★★☆☆ ⏱ 15 min

After mapping your route, you need to specify the correct reagents and conditions for every step. CIE marking schemes award heavy marks for correct conditions, so they must not be omitted.

3. Planning a Full 3-Step Synthetic Route ★★★★☆ ⏱ 20 min

To plan a full forwards route, combine the results of your retrosynthetic analysis with your knowledge of reagents. Always check that existing functional groups are not affected by each step, and adjust the order of reactions if needed.

Exam tip: Always write reagents and conditions clearly for every step, even if the step seems obvious

4. Evaluating Alternative Synthetic Routes ★★★★☆ ⏱ 15 min

CIE questions often ask you to select the best route from multiple options. Evaluate routes based on these key criteria:

  • Overall yield: Fewer steps generally give higher yield, but high-yield multiple steps are better than low-yield single steps
  • Side reactions: Routes that avoid unwanted reactions at other functional groups are preferred
  • Cost: Cheaper starting materials and reagents are better
  • Safety: Less toxic reagents are preferred
  • Purity: Routes that produce easily purified product are better

Common Pitfalls

Why: Examiners expect correct notation to demonstrate understanding of backwards planning

Why: Without reflux and excess oxidant, only the aldehyde intermediate will form

Why: CIE marking schemes award 1 mark per step for correct conditions, which are easy marks to lose

Why: A one-step reversible route with low yield is worse than a two-step route with high yield per step

Why: Oxidising agents will react with double bonds and alcohols, leading to unwanted side products

Quick Reference Cheatsheet

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